$Bruker apex iidiffractometer$

It also incorporates a new goniometer with an enhanced interface, all enclosed in a fail. This system is completely redesigned and features a new CCD detector, based upon a 4K CCD chip. = Resolution & Completeness Statistics (Cumulative) = Theta sin(th)/Lambda Complete Expected Measured Missing -РІР‚вЂњ 20.82 0.500 0.982 397 390 7 23.01 0.550 0.986 500 493 7 25.24 0.600 0.989 650 643 7 - ACTA Min. 1.1 SMART APEX Features The Bruker AXS SMART APEX system is the newest member the SMART CCD product line of instrumentation for single crystal X-ray diffraction. Between TH(Min) & STH/ L=0.6 6 912_ALERT_3_C # Missing FCF Reflections Above STH/ L=0.6 # 1 C6 H12 N2 O4 S2Р”В©10_ALERT_3_C # Missing FCF Reflections Below TH(Min) 6 790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.293 KР”В¬onfirm: This determination was performed at room temperature.Р”Р€40_ALERT_3_C Low Bond Precision on C-C bonds ( x 1000) Ang

$bruker apex iidiffractometer$

This symbol was pasted from the PLATON Chk file.Р”РЋ99_ALERT_1_C Check the Reported _cell_measurement_temperature 293 K 200_ALERT_1_C Check the Reported _diffrn_ambient_temperature. 31 XRD data collection for compound 4, 5, 6 were was carried out on the. Empirical absorption corrections were applied using SADABS or TWINABS.

$bruker apex iidiffractometer$

The absolute structure was known prior to data collection.Р”РЋ27_ALERT_1_C Implicit Hall Symbol Inconsistent with Explicit P 61 2 (0 0 5) XRD data collections for compound 1 and 8 was performed on a Bruker APEX II diffractometer with use of an Incoatec microfocus sealed tube of Mo K radiation (0.71073 Р“вЂ¦) and a CCD area detector. The effects of pressure can be interpreted in terms of closing-up of voids in the structure, and this leads to (i) a lessening of the N-C-C-O and C-S-S-C torsional angles, (ii) shortening of the N-H O hydrogen bonds by 0.10-0.60Р’В Р“вЂ¦ and (iii) a further shortening of an already short S S contact from 3.444Р’В (4)Р’В Р“вЂ¦ to 3.264Р’В (4)Р’В Р“вЂ¦.Р”В 34_ALERT_1_C No Flack Parameter Given. The compression occurs approximately equally in the regions of the interlayer hydrogen bonds and the disulfide bridges in the latter, changes in the C-S-S-C torsion angles allow the cystine molecules to act like springs. The most compressible unit-cell dimension, and the direction of greatest strain in the structure, is along the c-axis, and application of pressure pushes the layers closer together. These layers are connected on one side by the disulfide bridges within the cystine molecules, and on the other by NH O hydrogen bonds to other glycine-like layers. The structure consists of hydrogen-bonded layers which are strongly reminiscent of those seen in -glycine, and consist of (16) hydrogen-bonded ring motifs. The crystals were mounted on a cryoloop under Paratone-N oil and kept under nitrogen. The structure of this phase consists of molecules in their zwitterionic form, and crystallizes in the hexagonal space group P6 122. collected on a Bruker KAPPA APEX II diffractometer equipped with an APEX II CCD detector using a TRIUMPH monochromator with a Mo K X-ray source ( 0.71073 Р“вЂ¦). The crystal structure of hexagonal L-cystine has been determined at room temperature at pressures between 0.4 and 3.7Р’В GPa unit-cell dimensions were measured up to 6.4Р’В GPa. Diffraction data was collected, at room temperature, with a Bruker APEX II diffractometer on single crystal of 0.2, 0.1 and 0.02mm 3 dimensions at room temperature with MoKa radiation and a graphite monochromator.

$Bruker apex iidiffractometer$